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Haraga, Tomoko; Kameo, Yutaka; Nakashima, Mikio
Bunseki Kagaku, 55(1), p.51 - 54, 2006/01
Times Cited Count:4 Percentile:14.43(Chemistry, Analytical)A relatively large quantity of sample solutions have to be prepared for radiochemical analysis of solidified products yielded by plasma melting treatment of non-metallic radioactive wastes. In order to dissolve the solidified products sample rapidly, dissolution method with microwave heating devices was applied. In a conventional method only by external heating with various mixtures of acids (HNO, HF, HClO and HSO), a 0.1 g amount of the sample was dissolved with difficulty. However, applying the microwave assisted dissolution method, a 1 g amount of the sample was completely dissolved in a shorter time. Thereby the time for dissolution procedures was shortened less than a one-tenth. The present dissolution method was successfully applied to the blast furnace slag as a reference material to determine main elements with good precision.